مقایسه‌‌‌‌‌‌ی بازده سامانه توأم فراصوت- کلونجر و سامانه کلونجر در استخراج اسانس انیسون

نوع مقاله : مقاله پژوهشی

نویسندگان

1 گروه فنی کشاورزی - پردیس ابوریحان - دانشگاه تهران - تهران - ایران

2 مرکز تحقیقات گیاهان دارویی- دانشکده داروسازی – دانشگاه علوم پزشکی تهران - تهران - ایران

3 گروه بیوسیستم فنی کشاورزی - پردیس ابوریحان - دانشگاه تهران - تهران - ایران

10.22034/fr.2025.67500.1967

چکیده

در این تحقیق استخراج اسانس از بذر گیاه انیسون به روش تقطیر با آب همزمان با اعمال امواج فراصوت (فراصوت-کلونجر) و روش مرسوم تقطیر با آب به تنهایی (کلونجر) صورت پذیرفت. نتایج بدست آمده از نظر بازده استخراج، انرژی مصرفی و خواص فیزیکی و شیمیایی مورد مقایسه قرار گرفت. برای این منظور آزمایش‌ها در سه سطح توان فراصوت (200، 350 و 500 وات)، سه سطح زمان اعمال فراصوت (20، 40 و 60 دقیقه) و روش موج دهی فراصوت (پیوسته، 2 ثانیه خاموش- 2 ثانیه روشن و 4 ثانیه خاموش-2 ثانیه روشن) در فرکانس ثابت 20 کیلو هرتز انجام شد. روش استخراج اسانس با استفاده از کلونجر در مدت زمان 180 دقیقه و دمای جوش نیز به عنوان شاهد در نظر گرفته شد. نتایج نشان داد که طبق شرایط بهینه، نقطه‌ی بهینه در زمان 20 دقیقه، توان 200 وات و موج‌دهی 4 ثانیه خاموش- 2 ثانیه روشن ،با حداقل مصرف انرژی و کاهش 1/4 دقیقه‌ای زمان، فرآیند استخراج اسانس انیسون تکمیل شد. استفاده از سامانه‌ی فراصوت- کلونجر به میزان قابل توجهی زمان استخراج اسانس را کاهش داده و همچنین در کاهش مصرف انرژی نقش مهمی را دارد. در ترکیبات اسانس استخراج شده در شرایط مختلف توسط کروماتوگرافی گازی- طیف سنجی جرمی، تفاوت‌هایی در نوع و میزان ترکیبات مشاهده شد، به طوری که بیشترین درصد آنتول از مهمترین ترکیب موجود در اسانس انیسون ، در نمونه‌های تحت تیمار فراصوت- کلونجر بوده و همچنین این روش در استخراج ترکیبات استراگول، گاما هیماچالین ( ترکیب طبیعی از خانواده سزکویی ترپن)و زینجیبرن (سزکویی ترپن اصلی موجود در اسانس زنجبیل) نسبت به روش کلونجر برتری داشت.

کلیدواژه‌ها

موضوعات


عنوان مقاله [English]

omparison of the efficiency of combined Sono-Clevenger system and Clevenger system in extracting Pimpinella anisum essential oil

نویسندگان [English]

  • Mir Mohammad Mousavi 1
  • Mohammad Aboonajmi 1
  • saeed Goodarzi 2
  • Akbar Arabhosseini 3
1 Department of Agrotechnology, College of Aburaihan,, University of Tehran, Tehran, Iran
2 Medicinal Plants Research Center, Faculty of Pharmacy, Tehran University of Medical Sciences, Tehran, Iran
3 - Department of Agrotechnology, ,College of Aburaihan, University of Tehran, Tehran, Iran
چکیده [English]

In this research, extraction of essential oil from the seeds of anise plant was done by the method of distillation with water simultaneously with the application of ultrasound waves (Sono-Clevenger) and the conventional method of distillation with water (Clevenger). The obtained results were compared in terms of extraction efficiency, energy consumption and physical properties. For this purpose, were conducted at three levels of ultrasound power (200, 350 and 500 watts), three levels of ultrasound application time (20, 40 and 60 minutes) and three modes of ultrasound of waves (continuous, 2 seconds off-2 seconds on and 4 seconds off-2 seconds on) and fixed frequency of 20. The method of extracting the essential oil using clevenger in a period of 180 minutes and boiling temperature was also considered as a control. The results showed that according to the optimal conditions estimated by the software, the optimal point was a complete extraction of Anise essential oil in 20 minutes with 200 watts of power and 4 seconds off - 2 seconds on mode, while the extraction time reduced about ¼ times. The use of the Sono-Clevenger system significantly reduces the duration of essential oil extraction and also plays an important role in reducing energy consumption. In the given essential oil compounds that were analyzed by GC-MS, the highest percentage of anthole, which is the most important one in the anise essential oil, was in the samples that were subjected to Sono-Clevenger, as well as Sono-Clevenger in estragole compounds, gamma.-himachalene and Zingiberene was superior to Clevenger's method.

In this research, extraction of essential oil from the seeds of anise plant was done by the method of distillation with water simultaneously with the application of ultrasound waves (Sono-Clevenger) and the conventional method of distillation with water (Clevenger). The obtained results were compared in terms of extraction efficiency, energy consumption and physical properties. For this purpose, were conducted at three levels of ultrasound power (200, 350 and 500 watts), three levels of ultrasound application time (20, 40 and 60 minutes) and three modes of ultrasound of waves (continuous, 2 seconds off-2 seconds on and 4 seconds off-2 seconds on) and fixed frequency of 20. The method of extracting the essential oil using clevenger in a period of 180 minutes and boiling temperature was also considered as a control. The results showed that according to the optimal conditions estimated by the software, the optimal point was a complete extraction of Anise essential oil in 20 minutes with 200 watts of power and 4 seconds off - 2 seconds on mode, while the extraction time reduced about ¼ times. The use of the Sono-Clevenger system significantly reduces the duration of essential oil extraction and also plays an important role in reducing energy consumption. In the given essential oil compounds that were analyzed by GC-MS, the highest percentage of anthole, which is the most important one in the anise essential oil, was in the samples that were subjected to Sono-Clevenger, as well as Sono-Clevenger in estragole compounds, gamma.-himachalene and Zingiberene was superior to Clevenger's method.
In this research, extraction of essential oil from the seeds of anise plant was done by the method of distillation with water simultaneously with the application of ultrasound waves (Sono-Clevenger) and the conventional method of distillation with water (Clevenger). The obtained results were compared in terms of extraction efficiency, energy consumption and physical properties. For this purpose, were conducted at three levels of ultrasound power (200, 350 and 500 watts), three levels of ultrasound application time (20, 40 and 60 minutes) and three modes of ultrasound of waves (continuous, 2 seconds off-2 seconds on and 4 seconds off-2 seconds on) and fixed frequency of 20. The method of extracting the essential oil using clevenger in a period of 180 minutes and boiling temperature was also considered as a control. The results showed that according to the optimal conditions estimated by the software, the optimal point was a complete extraction of Anise essential oil in 20 minutes with 200 watts of power and 4 seconds off - 2 seconds on mode, while the extraction time reduced about ¼ times. The use of the Sono-Clevenger system significantly reduces the duration of essential oil extraction and also plays an important role in reducing energy consumption. In the given essential oil compounds that were analyzed by GC-MS, the highest percentage of anthole, which is the most important one in the anise essential oil, was in the samples that were subjected to Sono-Clevenger, as well as Sono-Clevenger in estragole compounds, gamma.-himachalene and Zingiberene was superior to Clevenger's method.
In this research, extraction of essential oil from the seeds of anise plant was done by the method of distillation with water simultaneously with the application of ultrasound waves (Sono-Clevenger) and the conventional method of distillation with water (Clevenger). The obtained results were compared in terms of extraction efficiency, energy consumption and physical properties. For this purpose, were conducted at three levels of ultrasound power (200, 350 and 500 watts), three levels of ultrasound application time (20, 40 and 60 minutes) and three modes of ultrasound of waves (continuous, 2 seconds off-2 seconds on and 4 seconds off-2 seconds on) and fixed frequency of 20. The method of extracting the essential oil using clevenger in a period of 180 minutes and boiling temperature was also considered as a control. The results showed that according to the optimal conditions estimated by the software, the optimal point was a complete extraction of Anise essential oil in 20 minutes with 200 watts of power and 4 seconds off - 2 seconds on mode, while the extraction time reduced about ¼ times. The use of the Sono-Clevenger system significantly reduces the duration of essential oil extraction and also plays an important role in reducing energy consumption. In the given essential oil compounds that were analyzed by GC-MS, the highest percentage of anthole, which is the most important one in the anise essential oil, was in the samples that were subjected to Sono-Clevenger, as well as Sono-Clevenger in estragole compounds, gamma.-himachalene and Zingiberene was superior to Clevenger's method.
In this research, extraction of essential oil from the seeds of anise plant was done by the method of distillation with water simultaneously with the application of ultrasound waves (Sono-Clevenger) and the conventional method of distillation with water (Clevenger). The obtained results were compared in terms of extraction efficiency, energy consumption and physical properties. For this purpose, were conducted at three levels of ultrasound power (200, 350 and 500 watts), three levels of ultrasound application time (20, 40 and 60 minutes) and three modes of ultrasound of waves (continuous, 2 seconds off-2 seconds on and 4 seconds off-2 seconds on) and fixed frequency of 20. The method of extracting the essential oil using clevenger in a period of 180 minutes and boiling temperature was also considered as a control. The results showed that according to the optimal conditions estimated by the software, the optimal point was a complete extraction of Anise essential oil in 20 minutes with 200 watts of power and 4 seconds off - 2 seconds on mode, while the extraction time reduced about ¼ times. The use of the Sono-Clevenger system significantly reduces the duration of essential oil extraction and also plays an important role in reducing energy consumption. In the given essential oil compounds that were analyzed by GC-MS, the highest percentage of anthole, which is the most important one in the anise essential oil, was in the samples that were subjected to Sono-Clevenger, as well as Sono-Clevenger in estragole compounds, gamma.-himachalene and Zingiberene was superior to Clevenger's method.
In this research, extraction of essential oil from the seeds of anise plant was done by the method of distillation with water simultaneously with the application of ultrasound waves (Sono-Clevenger) and the conventional method of distillation with water (Clevenger). The obtained results were compared in terms of extraction efficiency, energy consumption and physical properties. For this purpose, were conducted at three levels of ultrasound power (200, 350 and 500 watts), three levels of ultrasound application time (20, 40 and 60 minutes) and three modes of ultrasound of waves (continuous, 2 seconds off-2 seconds on and 4 seconds off-2 seconds on) and fixed frequency of 20. The method of extracting the essential oil using clevenger in a period of 180 minutes and boiling temperature was also considered as a control. The results showed that according to the optimal conditions estimated by the software, the optimal point was a complete extraction of Anise essential oil in 20 minutes with 200 watts of power and 4 seconds off - 2 seconds on mode, while the extraction time reduced about ¼ times. The use of the Sono-Clevenger system significantly reduces the duration of essential oil extraction and also plays an important role in reducing energy consumption. In the given essential oil compounds that were analyzed by GC-MS, the highest percentage of anthole, which is the most important one in the anise essential oil, was in the samples that were subjected to Sono-Clevenger, as well as Sono-Clevenger in estragole compounds, gamma.-himachalene and Zingiberene was superior to Clevenger's method.

کلیدواژه‌ها [English]

  • Essential oil
  • Anise
  • Ultrasound
  • Sono-clevenger
  • Extraction
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